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Packed Bed Distillation Column

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Packed Bed Distillation Column

Packed Bed Distillation Column
 
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Product Details:
Reflux DividerSpecial arrangement to change R/D ratio automatically.
RotameterFor cooling water flow rate measurement
CondenserShell & Tube type made of Stainless Steel.
Distillate tank:Made of Stainless Steel,capacity 5Ltrs.
HeatersMade of Stainless Steel,capacity 5Ltrs. Nichrome wire heater.
Temperature SensorsRTD PT-100 type

The column is made of Stainless Steel material packed with Packed Bed Distillation Column. An electrically heated re-boiler is installed at the bottom of the column. The bottom product is collected in the tank. The vapours form the top of column are condensed in the shell and tube type condenser by circulating cooling water, supplied by laboratory overhead tank. The condensate is divided into reflux and distillate by automatic reflux divider and R/D Ratio can be varied. Reflux is fed back to the column and distillate is received in a receiving tank. The complete column is insulated for minimizing the heat loss. Instrumentation is provided for pressure & temperature measurement wherever necessary.

Learning Objectives/Experiments:
  • To estimate the batch distillation curves for a binary system and verify the binary batch distillation equation for a known packed height.
  • To operate the column under total reflux condition and estimate the HETP for the packing.

Required for Operation:
  • Required Chemicals.
  • Refractometer for analysis.
  • Steam Generator: Made of Stainless Steel, provided with Pressure Gauge Level Indicator, Safety Valve & insulated with ceramic wool and Cladding with Aluminum foil.
  • The whole set-up is ingeniously designed and schematically arranged on a powder-coated rigid structure.

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • Digital Temp. Controller 0-199.9 DegreeC, For Re-boiler.
  • Digital Temp. Indicator 0-199.9 DegreeC, with multi-channel switch.

Scope of Delivery:
  • 1 Self-contained 'Packed Bed Distillation Column' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-08
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