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Bubble Cap Distillation Column

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Bubble Cap Distillation Column

Bubble Cap Distillation Column
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Product Details:
MaterialStainless Steel
Temperature Sensors typeRTD PT-100
CondenserShell & Tube type made of Stainless Steel
Distillation Column diameter110mm
HeaterNichrome wire heater.
Bottom product tank capacity5 Ltrs
Distillate tank capacity5 Ltrs
Pressure GaugeBourdon type
Reflux DividerSpecial arrangement to change R/D ratio automatically.
RotameterFor cooling water flow rate measurement. Indicator,Safety valve
Water Supply2 LPM at 5 m head.
Electricity Supply1 Phase,220 V AC,6 kW

The column is made of Stainless Steel with seven plates for mounting the bubble caps. Each plate is provided with one bubble cap. An electrically heated reboiler is installed at the bottom of the column. The bottom product is collected in the tank. The vapours form the top of column are condensed in the shell and tube type condenser by cooling water supplied by laboratory overhead tank. The condensate is divided into reflux and distillate by automatic reflux divider and R/D Ratio can be varied. Reflux is fed back to the column and distillate is received in a receiving tank. The complete column is insulated for minimizing the heat loss. Instrumentation provided for pressure & temperature measurement wherever necessary.

Learning Objectives/Experiments:
  • To estimate the batch distillation curves for a binary system and verify the binary batch distillation equation for a known number of theoretical plates.
  • To operate the column under total reflux condition and estimate the minimum number of theoretical plates required.

Required for Operation:
  • Drain.
  • Required Chemicals.
  • Refractometer for analysis

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • 0-199.9 DegreeC, For Reboiler.
  • 0-199.9oC, with multi-channel switch

Scope of Delivery:
  • 1 Self-contained 'Bubble Cap Distillation Column' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-06
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Plot No. 46/19/2, Near Bala Sundri Mandir, Herman City Road, Chotta Khudda, Ambala Cantt, Ambala - 133001, Haryana, India
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