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Ambala, Haryana
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Mass Transfer Lab equipment

  • Extraction
  • Absorption & diffusion
  • Distillation
  • Drying & Crystallization
  • Miscellaneous
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Packed Bed Type Solid Liquid Extraction Apparatus

Packed Bed Type Solid Liquid Extraction Apparatus
 
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Product Details:
Temperature SensorRTD PT-100 Type.
Electricity Supply1 Phase, 220 V AC, 1.5 kW
Solvent circulationMagnetic Pump made of Polypropylene to Circulate solvent.
Extraction ColumnMaterial Borosilicate Glass.
Solvent Flow MeasurementRota Meter
Solvent TankMade of Stainless Steel, Capacity 30 Ltrs. Double wall.
Digital Temp. Controller0-199.9 deg C (For Hot Water Bath)
HeaterNichrome wire heater

We are among the leading manufacturers, suppliers and exporters of Solid Liquid Extraction Packed Bed Type to our valuable customers. This apparatus is precisely designed from premium quality stainless steel, which is procured from well known vendors. The offered apparatus is commonly used for performing various solid liquid extractions that are used in different sample preparation in lab.

Technical Description:
  • This setup is designed to study the performance characteristics of solvent extraction of a particular component from a packed bed of solid material. The apparatus allows study of such systems as water/inorganic salts, water/sugar bed, methylene chloride/vegetable oil etc. The glass column is fitted with SS mesh to support the solid material. The solvent is introduced near the bottom of the column and it flows upward counter-currently to the solids. A pump supplies the solvent and flow rate is monitored by means of a Rota meter. Solvent feed tank is kept in a bath fitted with heater and digital temperature controller is used to maintain the constant temperature

Learning Objectives/Experiments:
  • To study the effect of various system parameters like, solvent temperature, solvent rate and particle size on the %age recovery of oil from solid.

Required for Operation:
  • Solvent: 30ltrs.
  • Solid: 10kg
  • Table for setup support

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.

Scope of Delivery:
  • 1 Self-contained 'Solid Liquid Extraction Packed Bed Type' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-05
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Rotary Dryer

Rotary Dryer
 
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Product Details:
Floor space1.5 m x 2 m
Electricity Supply1 Phase, 220 V AC, 4 kW
Feed HopperMaterial Stainless Steel, Compatible Capacity
Hot Air CirculationBy forced draft fan, Arrangement is done to vary the air flow rate.
Drying ShellMaterial Stainless Steel, Length 1.5 m, Dia 110 mm.
HeaterNichrome wire heater
Heating ChamberCompatible capacity
Temperature SensorsRTD PT-100 type.
Product ReceiverMaterial Stainless Steel, Compatible Capacity.
Rotating ActionUsing motor coupled with a Reduction Gear Box.
DesignCustomized

Owing to the vast experience and knowledge of this field, we have been able to offer premium quality Rotary Dryer to our esteemed customers. Manufactured in compliance with the industry laid standards, this apparatus is commonly used for various drying purposes. The offered dryers are known for their hassle free operations and easy maintenance.

Technical Description:
  • Rotary dryer is a unit in which drying is done by forced draft action created by hot air. The set-up consists of a long revolving cylindrical shell slightly inclined towards the outlet. The shell is fitted with two brackets for support. Air from a blower passes through a heating chamber serves the purpose of drying agent. An arrangement for rotating the dryer shell at low RPM is provided by means of an electrical motor and a reduction gearbox. Wet feed enters from one end of the cylinder and dry material discharges from the other end. As the shell rotates internal flights lift the solids and shower them down through the interior of the shell. This action increases the contact of wet solid against hot air making the dryer very effective. The flow of hot air is counter-current to solids. Flow control and by-pass valve are fitted to regulate the airflow.

Learning Objectives/Experiments:
  • To study the operation of a Rotary Dryer.
  • To study the drying characteristics of a solid material under batch drying condition in a rotary dryer.

Required for Operation:
  • Wet Solid.

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • Digital Temp. Controller 0-199.9 DegreeC (For Hot Air).

Scope of Delivery:
  • 1 Self Contained "Rotary Dryer" Apparatus.
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-18
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Natural Draft Tray Dryer

Natural Draft Tray Dryer
 
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Product Details:
Electricity Supply1 Phase, 220 V AC, 2 kW.
Weighing BalanceDigital, 0-1000gm. of +- 1 gm resolution.
HeaterNichrome wire heater
Temperature SensorRTD PT-100 type
Maximum Temperature120 degree C
Drying Chamber Material Size30 x 30 x 30 cm
MaterialStainless Steel insulated by Ceramic wool and housed in a MS Chamber.

Owing to the vast experience and knowledge of this field, we have been able to offer premium quality Natural Draft Tray Dryer to prestigious customers. These dryers are commonly used for analyzing the moisture elimination by various condition of high temperature under natural draft action. This draft action is generated by the hot stream of air.

Technical Description:
  • Natural Draft Tray Dryer is a dryer in which moisture removal takes place by heat under natural condition. The set-up consists of an insulated Stainless Steel chamber fitted with heater. Inside the chamber a tray is attached directly to an electronic weighing balance, which is fitted on the bottom, outside the chamber. Material for drying is placed in the tray and regular loss of weight is monitored. Temperature controller fitted in the set-up maintains the required temperature in the chamber.

Learning Objectives/Experiments:
  • To study the drying characteristics of a solid material under batch drying condition.
  • Determination of drying rate and to plot moisture lost with time under for different operating conditions.

Required for Operation:
  • Drying Solids.
  • Table for setup support

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • Digital Temp. Controller 0-199.9 Degree C for Drying Chamber.

Scope of Delivery:
  • 1 Self Contained 'Natural Draft Tray Dryer' Apparatus.
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-16
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Forced Draft Tray Dryer

Forced Draft Tray Dryer
 
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Product Details:
Weighing BalanceDigital (0-1000gm) of +- 1 gm resolution.
Hot Air CirculationBy forced draft fan, Arrangement is done to vary the air flow rate.
Size20 x 20 x 25 cm
Electricity Supply1 Phase, 220 V AC, 2.5 kW
Temperature SensorsRTD PT - 100 Type
Heating ChamberCompatible capacity.
Drying ChamberInsulated double wall chamber

Our organization holds expertise in offering premium quality Forced Draft Tray Dryer to our valuable customers. Manufactured as per the industry set standards, these forced draft tray dryers are widely used for the purpose of analyzing the rate of drying of wet sawdust. The offered analyzing is performed under a wide range of different temperature conditions.

Technical Description:
  • Forced Draft Tray Dryer is a dryer in which moisture removal takes place by means of forced draft action created by hot air. The set-up consists of an insulated double wall chamber. Inside the chamber a tray is attached directly to a electronic weighing balance, which is fitted on the bottom, outside the chamber. Material for drying is placed in the tray and regular loss of weight is monitored. Air from a blower passes through a heating chamber and is used as drying agent. Arrangement is done to vary the airflow rate.

Learning Objectives/Experiments:
  • To study the drying characteristics of a solid under forced draft condition and determine the critical moisture content.
  • To correlate the constant drying rate with air mass velocity.

Control Panel:
  • Digital Temp. Indicator: 0-199.9 DegreeC (with multi-channel switch)
  • Standard make on/off switch, Mains Indicator etc.

Scope of Delivery:
  • Self-contained 'Forced Draft Tray Dryer' Apparatus
  • Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-17
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Adsorption in Packed Bed Apparatus

Adsorption in Packed Bed Apparatus
 
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Product Details:
Minimum Order Quantity1 Piece
Feed tankMaterial Stainless Steel, Capacity 20 litres
PipingStainless Steel and PVC
Capacity20 litres
Size1/4 Inch
Flow measurementRotameter for feed.
Column (3 Nos)Material Borosilicate glass of different dia.
Stop WatchElectronic
Feed circulationFHP, Magnetic Pump made of Polypropylene

Owing to the rich experience and knowledge of this field, we have been able to offer optimum quality Adsorption in Packed Bed Apparatus to our valuable customers. The offered apparatus is commonly used for determining the process of adsorption in packed bed arrangement. Due to the hassle free installation and simple construction, these apparatus is highly demanded in the market.

Technical Description:
  • The set up consist of three vertical column packed with activated Charcoal. Columns are operated individually. Liquid feed with dye is fed to the individual column from the bottom and samples are collected from the top at regular interval of time. Rotameter is provided to measure the flow rate. Pump with a feed tank is provided for fluid flow.

Learning Objectives/Experiments:
  • To obtain the breakthrough curve and hence length of unused bed for the given adsorption system.

Required for Operation:
  • Electricity Supply: 1 Phase, 220 V AC, 0.5 kW
  • Bench Area: 1.2m x 1m.
  • Required Chemicals & Laboratory Glassware.
  • Colorimeter. Required analyzing equipments as per the system to study.

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.

Scope of Delivery:
  • 1 Self-contained 'Adsorption in Packed Bed Apparatus' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-26
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Batch Crystallizer

Batch Crystallizer
 
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Product Details:
Cooling Water Tank Capacity30 L
StirrerFHP, Variable Speed.
Cooling Water Tank MaterialStainless Steel
Crystallizer (Jacketed Type) Capacity2Ltrs.
Electricity Supply1 Phase, 220 V AC, 1.5 kW
Crystallizer (Jacketed Type) MaterialStainless Steel
Stainless Steel Capacity2 L
Receiving Tank MaterialStainless Steel , Capacity 2litre with SS sieve.
Crystallizer (Jacketed Type)Material Stainless Steel, Cap. 2Ltrs. with conical bottom.
Cooling Water TankMaterial Stainless Steel , Capacity 30litre fitted with Pump.
Flow measurementRotameter
PumpFHP
Temperature SensorsRTD PT-100 type
HeaterNichrome wire heater

Batch Crystallizer is the formation of solid particles within a homogeneous phase of saturated liquid. Its wide use has a two-fold basis, a crystal formed from an impure solution is itself pure and crystallization affords a practical method of separating w. This operation involves both heat and mass transfer. Cooling type agitated batch crystallizer set up consists of an open jacketed stirred vessel provided with water heating & cooling arrangement. The feed is prepared in the crystallizer itself with hot water and stirrer. The hot saturated solution in the crystallizer is then cooled by circulation of cooling water and crystals are formed.

Learning Objectives/Experiments:
  • To study the performance of a Batch Crystallizer.
  • To determine the crystal yield and the efficiency of crystallizer.

Required for Operation:
  • Water Supply.
  • Drain.
  • Required Chemicals

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • Digital Temp. Indicator 0-199.90C with multi-channel switch.

Scope of Delivery:
  • 1 Self Contained "Batch Crystallizer" Apparatus.
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-20
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Mass Transfer with & without Chemical Reaction Apparatus

Mass Transfer with & without Chemical Reaction Apparatus
 
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Product Details:
Instruction ManualAn English instruction manual will be provided along with the Apparatus
Temperature SensorsRTD PT-100 type
Water BathMaterial Stainless Steel, Double Wall,nsulated with ceramic fibre wool.
Electricity Supply1 Phase, 220 V AC, 0.5 kW
StirrerStainless Steel Impeller and shaft coupled with DC motor drive for variable speed
RPM IndicatorDigital, Non contact type. Digital Temp. Controller: 0-199.90C for hot water tank.
HeaterNichrome Wire Heater
ReactorMaterial Stainless Steel, Capacity 2 Ltrs. (approx)

The setup consists of a Reactor, in which solid cylinder of Benzoic Acid is placed and is stirred by means of a variable speed mixer. Baffles are also provided. The Reactor is made of Stainless Steel. Peltilizer is provided to make the solid cylinder of Benzoic Acid. Constant temperature water bath arrangement is provided to conduct the experiment at various temperatures.

Experimentation:
  • Dissolution of Benzoic acid in water: Kinetic studies
  • Dissolution of Benzoic acid with reaction in aqueous NaOH solution.

Utilities Required:
  • Water Supply
  • Drain
  • Instruments, Laboratory Glassware and Chemicals required for analysis as per the system adopted

Additional Information:
  • Item Code: QMT-24
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Vapour- Liquid Equilibrium Set- Up Apparatus

Vapour- Liquid Equilibrium Set- Up Apparatus
 
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Product Details:
HeaterNichrome wire
Temperature SensorsRTD PT-100 type
Capacity1 L
Distillation Still MaterialStainless Steel
Cooling Water Tank Capacity15 Ltrs.
Condenser typeConcentric Tube
MaterialStainless Steel

The basic data of any distillation problem are the equilibrium between the liquid and vapours phases of the system subjected to distillation. Hence is of great importance to study the vapour liquid equilibrium. The set-up consists of distillation still with a heating element. An electrical Dimmer stat is connected to heating element for varying heat input. The vapours form the top of column is condensed in the shell and tube type condenser by circulating cooling water. The condensate is collected in reflux drum and feedback to column as reflux. A tank with pump is provided to circulate cold water to condenser. Flow rates can be regulated through control valve fitted. Instrumentation is provided to measure the temperatures at different points

Learning Objectives/Experiments:
  • To determine the vapour Liquid Equilibrium curve for CCl4 and Toluene or any other mixture.

Required for Operation:
  • Water Supply.
  • Drain.
  • Refractrometer for Analysis.
  • Required Chemicals

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.Digital Voltmeter: 0-300 Volt.Dimmer stat: 0-230 V, 2A.Digital Temp. Indicator: 0-199.90C RTD PT-100 Type.

Scope of Delivery:
  • 1 Self-contained 'Vapour-Liquid Equilibrium Set-Up' Apparatus1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-23
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Wetted Wall Column Apparatus

Wetted Wall Column Apparatus
 
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Product Details:
Water CirculationFHP Pump
Electricity Supply1 Phase, 220 V AC, 0.5 kW
Digital Temp. Indicator0-199.90C, RTD PT-100 type with multi-channel switch. Standard make on/off switch, Mains Indicator
Instruction ManualAn ENGLISH instruction manual will be provided along with the Apparatus
Heating Chamber capacityCompatible
Dry & wet Bulb TempWith Digital Temperature Indicator.
Water Tank MaterialStainless Steel
Water Tank Capacity20 Litres
ColumnBorosilicate Glass Dia 45 mm, Length 1000 mm (approx.)
RotameterFor water flow rate measurement.
Temperature SensorsRTD PT-100 Type.
HeaterNichrome Wire Heater

The set up consists of a glass column. Water is fed at the top of the column along the walls to make the column a Wetted Wall Column. Hot air from heating chamber with known humidity is allowed to pass through the column vertically upward and evaporation in the liquid film around the wall takes place. The flow rates of water and air can be independently varied to simulate different conditions. Instrumentation is provided to measure the dry and wet bulb temperatures at air inlet and outlet.

Experimentation:
  • To determine the gas film coefficient in a wetted wall column using air-water
  • system.
  • To find the mass transfer coefficient

Utilities Required:
  • Compressed Air Supply at 2 Bar, 4 CFM.
  • Water supply.
  • Drain.

Additional Information:
  • Item Code: QMT-22
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Sieve Plate Distillation Column Apparatus

Sieve Plate Distillation Column Apparatus
 
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Product Details:
Steam GeneratorMade of Stainless Steel, provided with Pressure Gauge & Level Indicator
Pressure GaugeBourdon type, 0-2 kg/cm2
CondenserShell & Tube type made of Stainless Steel.
Reflux DividerSpecial arrangement to change R/D ratio automatically.
Distillate TankMade of Stainless Steel, capacity 5 Ltrs.
HeatersNichrome wire heater.
Temperature SensorsRTD PT-100 type.
Distillation ColumnMaterial Stainless Steel, Dia 110mm, seven sieve trays
RotameterFor cooling water flow rate measurement.
Bottom Product TankMade of Stainless Steel, Capacity 5 Ltrs.
Design TypeCustomised

Column is made of Stainless Steel material with seven sieve trays. An electrically heated re-boiler is installed at the bottom of the column. The bottom product is collected in the tank. The vapours form the top of column are condensed in the shell and tube type condenser by cooling water supplied by laboratory overhead tank. The condensate is divided into reflux and distillate by automatic reflux divider and R/D Ratio can be varied. Reflux is fed back to the column and distillate is received in a receiving tank. The complete column is insulated for minimizing the heat loss. Instrumentation is provided for pressure & temperature measurement wherever necessary

Learning Objectives/Experiments:
  • To estimate the batch curves for a binary system and verify the binary distillation equation for a known number of theoretical plates.
  • To operate the column under total reflux condition and estimate the minimum number of theoretical plates required.

Required for Operation:
  • Water Supply 2 LPM at 5m head.
  • Drain.
  • Electricity Supply: 1 Phase, 220 V AC, 6 kW.
  • Required Chemicals.
  • Refractrometer for analysis

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • Digital Temp. Controller 0-199.9 DegreeC for Drying Chamber.
  • Digital Temp. Indicator 0-199.90C, (with multi-channel switch).

Scope of Delivery:
  • 1 Self Contained 'Sieve Plate Distillation Column Apparatus' Apparatus.
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-07
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Fluidized Bed Dryer

Fluidized Bed Dryer
 
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Product Details:
Electricity Supply1 Phase, 220 V AC, 3 kW.
Column MaterialBorosilicate Glass
Temperature SensorsRTD PT-100 type.
HeaterNichrome wire heater
Air CirculationBy forced draft fan, Arrangement is done to vary the air flow rate.
Column Diameter80 mm
Cyclone Separator MaterialStainless Steel
Heating ChamberCompatible capacity
Column Length500 mm

This is a dryer in which moisture removal takes place by Fluidized Bed Dryer by hot air. The set-up fitted with a specially designed, vertical Glass Column. The lower portion of the column is filled with fluidizing material. The material is supported on the screen mesh held between two flanges. Air from a compressor is heated in the heater box and passed through the column. Flow control and by-pass valve are fitted to regulate the airflow. At the top outlet of column a cyclone is provided to collect any solid particles taken out by the air stream.

Learning Objectives/Experiments:
  • To study the fluidized bed drying
  • To plot the drying curve under fluidized bed condition

Required for Operation:
  • Granular and free flowing solid of size 1 to 2 mm

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • Digital Temp. Controller 0 199.9 DegreeC

Scope of Delivery:
  • 1 Self Contained "Fluidized Bed Dryer" Apparatus.
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-19
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Liquid Liquid Extraction In A Packed Tower

Liquid Liquid Extraction In A Packed Tower
 
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Product Details:
Extraction Column Height750 mm (approx)
Feed Tanks Capacity20 Ltrs. (2 Nos.)
Extraction Column MaterialBorosilicate Glass
Instruction ManualAn English instruction manual will be provided along with the Apparatus
Extract & Raffinate TanksMaterial Stainless Steel, Cap 10 Ltrs.
Compressed Air Supply2 Bar, 0.5 CFM.
PackingRasching Rings, Material Borosilicate Glass
Extraction Column diameter55 mm
Feed Tanks MaterialStainless Steel
Feed CirculationBy Compressed Air
Flow MeasurementRotameters (One each for solvent & solute)

The set-up consists of a glass column packed with Rasching rings. Continuous counter current contacts between the solvent and solute phases is made, which results into extract and raffinate streams. Flow meters (Rotameters) are used to note the flow of solvent & solute respectively. The continuous and dispersed phase streams are metered and derived from separate containers. The total set-up is housed in a well-designed rigid structure. The structure also supports tanks, piping, Rotameters, panel and other units.

Experimentation:
  • To determine overall mass transfer co-efficient based on continuous & dispersed phase.
  • To determine individual "Height of Transfer Unit" based on continuous & dispersed phase.

Utilities Required:
  • Compressed Air Supply at 2 Bar, 0.5 cfm.
  • Water Supply
  • Drain.
  • Required Chemicals & Laboratory Glassware.

Additional Information:
  • Item Code: QMT-01
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Bubble Cap Distillation Column

Bubble Cap Distillation Column
 
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Product Details:
CondenserShell & Tube type made of Stainless Steel
Water Supply2 LPM at 5 m head.
Electricity Supply1 Phase, 220 V AC, 6 kW
Distillation Column diameter110mm
Distillate tank capacity5 Ltrs
HeaterNichrome wire heater.
RotameterFor cooling water flow rate measurement. Indicator, Safety valve
Pressure GaugeBourdon type
Temperature Sensors typeRTD PT-100
Bottom product tank capacity5 Ltrs
Reflux DividerSpecial arrangement to change R/D ratio automatically.
MaterialStainless Steel

The column is made of Stainless Steel with seven plates for mounting the bubble caps. Each plate is provided with one bubble cap. An electrically heated reboiler is installed at the bottom of the column. The bottom product is collected in the tank. The vapours form the top of column are condensed in the shell and tube type condenser by cooling water supplied by laboratory overhead tank. The condensate is divided into reflux and distillate by automatic reflux divider and R/D Ratio can be varied. Reflux is fed back to the column and distillate is received in a receiving tank. The complete column is insulated for minimizing the heat loss. Instrumentation provided for pressure & temperature measurement wherever necessary.

Learning Objectives/Experiments:
  • To estimate the batch distillation curves for a binary system and verify the binary batch distillation equation for a known number of theoretical plates.
  • To operate the column under total reflux condition and estimate the minimum number of theoretical plates required.

Required for Operation:
  • Drain.
  • Required Chemicals.
  • Refractometer for analysis

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • 0-199.9 DegreeC, For Reboiler.
  • 0-199.9oC, with multi-channel switch

Scope of Delivery:
  • 1 Self-contained 'Bubble Cap Distillation Column' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-06
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Absorption in Wetted Wall Column

Absorption in Wetted Wall Column
 
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Product Details:
Pressure GaugeBourdon type
Feed Tank Capacity20 Ltrs.
Column Height1000 mm (approx)
Feed Tank MaterialStainless Steel
Flow measurementRotameters
Collecting Tank Capacity10 Ltrs
Column materialBorosilicate Glass
Column Diameter45 mm
Compressed Air Supply2 Bar, 4 CFM.
Feed CirculationBy compressed air. (One each for feed, air & CO2).
Pressure Regulator0-2 kg/cm2
MaterialStainless Steel

We are indulged in offering Absorption in Wetted Wall Column to our clients. In compliance with set industry norms, our supervisors manufacture and design this product using supreme class material. It is corrosion resistant and gives optimum performance. It also has high strength and extended durability that makes the product super-efficient. Proper quality test is performed so as to ensure the performance of this product before dispatching.

Technical Description:
  • The set up consists of a glass column. Alkaline liquid is fed at the top of the column along the walls to create a laminar liquid flow along the walls of a wetted wall column. Flow rates of Air and Co2, are measured separately, mixed in a mixing chamber and then passed through the column vertically upward and absorbed in liquid film around the wall. All the flow rates can be independently varied to simulate different conditions. Liquid Sample can be taken out from the sampling point at the bottom of the column for analysis.

Learning Objectives/Experiments:
  • To determine the number of transfer units, Height of transfer unit and overall mass transfer co-efficient for the given system.

Required for Operation:
  • Water Supply
  • Floor Drain.
  • CO2 cylinder with control valve, pressure regulator and Pressure gauges
  • Required Chemicals & Laboratory Glassware.

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.

Scope of Delivery:
  • 1 Self-contained 'Absorption in Wetted Wall Column' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-13
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Packed Bed Distillation Column

Packed Bed Distillation Column
 
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Product Details:
RotameterFor cooling water flow rate measurement
CondenserShell & Tube type made of Stainless Steel.
Reflux DividerSpecial arrangement to change R/D ratio automatically.
HeatersMade of Stainless Steel, capacity 5Ltrs. Nichrome wire heater.
Temperature SensorsRTD PT-100 type
Distillate tank:Made of Stainless Steel, capacity 5Ltrs.

The column is made of Stainless Steel material packed with Packed Bed Distillation Column. An electrically heated re-boiler is installed at the bottom of the column. The bottom product is collected in the tank. The vapours form the top of column are condensed in the shell and tube type condenser by circulating cooling water, supplied by laboratory overhead tank. The condensate is divided into reflux and distillate by automatic reflux divider and R/D Ratio can be varied. Reflux is fed back to the column and distillate is received in a receiving tank. The complete column is insulated for minimizing the heat loss. Instrumentation is provided for pressure & temperature measurement wherever necessary.

Learning Objectives/Experiments:
  • To estimate the batch distillation curves for a binary system and verify the binary batch distillation equation for a known packed height.
  • To operate the column under total reflux condition and estimate the HETP for the packing.

Required for Operation:
  • Required Chemicals.
  • Refractometer for analysis.
  • Steam Generator: Made of Stainless Steel, provided with Pressure Gauge Level Indicator, Safety Valve & insulated with ceramic wool and Cladding with Aluminum foil.
  • The whole set-up is ingeniously designed and schematically arranged on a powder-coated rigid structure.

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • Digital Temp. Controller 0-199.9 DegreeC, For Re-boiler.
  • Digital Temp. Indicator 0-199.9 DegreeC, with multi-channel switch.

Scope of Delivery:
  • 1 Self-contained 'Packed Bed Distillation Column' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-08
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Spray Tower Apparatus

Spray Tower Apparatus
 
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Product Details:
Distillation ColumnMaterial Stainless Steel, Dia 110mm, seven sieve trays.
RotameterFor cooling water flow rate measurement.
Bottom Product TankMade of Stainless Steel, capacity 5Ltrs.
CondenserShell & Tube type made of Stainless Steel.
Pressure GaugeBourdon type, 0-2 kg/cm2.
Reflux DividerSpecial arrangement to change R/D ratio automatically.
Temperature SensorsRTD PT-100 type.
Distillate TankMade of Stainless Steel, capacity 5Ltrs.
HeatersNichrome wire heater.

The experimental set-up of Spray Tower consists of a glass column provided with necessary accessories. It operates in a semi-batch mode. The fine spray nozzle is fitted at the top. Feeds are metered by Rotameters and derived from separate feed tanks.

Learning Objectives/Experiments:
  • To study the effect of the dispersed phase flow rate on overall volumetric mass transfer coefficient.
  • Dispersed phase hold-up study.

Required for Operation:

  • Drain.
  • Required Chemicals & Laboratory Glassware.
  • Special arrangement for changing height of interface zone is done.
  • The whole set-up is ingeniously designed and schematically arranged on a powder-coated rigid structure.
  • Pressure Gauge: Bourdon type 0-2 kg/cm2
  • Feed Circulation: By Compressed Air
  • Pressure Gauge: Bourdon type 0-2 kg/cm2
  • Feed Circulation: By Compressed Air
  • Pressure Gauge: Bourdon type 0-2 kg/cm2
  • Feed Circulation: By Compressed Air

Control Panel:

  • Standard make On/Off switch, Mains Indicator etc.

Scope of Delivery:

  • 1 Self-contained ''Spray Tower'' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc

Technical Description:
Column is made of Stainless Steel material with seven sieve trays. An electrically heated re-boiler is installed at the bottom of the column. The bottom product is collected in the tank. The vapours form the top of column are condensed in the shell and tube type condenser by cooling water supplied by laboratory overhead tank. The condensate is divided into reflux and distillate by automatic reflux divider and R/D Ratio can be varied. Reflux is fed back to the column and distillate is received in a receiving tank. The complete column is insulated for minimizing the heat loss. Instrumentation is provided for pressure & temperature measurement wherever necessary

Learning Objectives/Experiments:

  • To estimate the batch curves for a binary system and verify the binary distillation equation for a known number of theoretical plates.
  • To operate the column under total reflux condition and estimate the minimum number of theoretical plates required.

Required for Operation:
  • Water Supply 2 LPM at 5m head.
  • Electricity Supply: 1 Phase, 220 V AC, 6 kW.
  • Required Chemicals.
  • Refractometer for analysis

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • Digital Temp. Controller 0-199.9°C for Drying Chamber.
  • Digital Temp. Indicator 0-199.90C, (with multi-channel switch).

Scope of Delivery:

  • 1 Self Contained ''Sieve Plate Distillation Column'' Apparatus.
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-03
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Absorption in Packed Bed Apparatus

Absorption in Packed Bed Apparatus
 
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Product Details:
ColumnBorosilicate Glass Dia. 55 mm, Length 750mm (approx.)
Flow measurementRota meters (One each for feed, air & CO2).
PackingBorosilicate Glass Reaching Ring
Feed CirculationBy compressed air.
Feed TankMaterial Stainless Steel, Capacity 20 Ltrs.
Collecting TankMaterial Stainless Steel, Capacity 10 Ltrs.
Pressure Regulator0-2 kg/cm2
Pressure GaugeBourdon type

Technical Description:
  • The set up consists of a glass column packed with Reaching rings. Liquid is fed at the top of the column through distributor. The solute gas and air are measured separately, mixed in a mixing chamber and then passed through the packed column vertically upward and absorbed in liquid. All the flow rates can be independently varied to simulate different conditions. Liquid sample can be taken out from the sampling point at the bottom of the column for analysis.

Learning Objectives/Experiments:
  • To determine the number of transfer units, Height of transfer unit and overall mass transfer co-efficient for the given system.

Required for Operation:
  • Compressed Air Supply at 2 Bar, 4 CFM.
  • Water Supply.
  • Floor Drain.
  • CO2 cylinder with control valve, pressure regulator and Pressure gauges.
  • Required Chemicals & Laboratory Glassware.

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.

Scope of Delivery:
  • 1 Self-contained 'Absorption in Packed Bed Apparatus' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-12
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York Scheibel's Extraction Unit

York Scheibel's Extraction Unit
 
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Product Details:
Feed Tank (2 Nos)Material Stainless Steel, Capacity 20 Ltrs.
Flow MeasurementRotameters (One each for solvent & solute)
AgitatorStainless Steel impellers with Stainless Steel shaft coupled to a Variable Speed DC Motor.
Pressure Regulator0-2 kg/cm2
Feed CirculationBy Compressed Air
Extraction ColumnMaterial Borosilicate Glass Dia. 45 mm, Height 750 mm (approx).
Extract & Raffinate TanksMaterial Stainless Steel, Capacity 10 Ltrs.
RPM MeasurementDigital RPM Indicator, non contact type with proximity sensor.
Pressure GaugeBourdon type, 0-2 kg/cm2
PackingWoven mesh of Stainless Steel

The York Scheibel's Column Apparatus in the class of gravity-operated extractors with mechanical agitation. The presence of alternatively agitating and calming sections in a York Scheibel's column yield higher extraction efficiency than the conventional packed column. In the setup a continuous counter current contact between the solvent and solute phases is made which results into extract and raffinate streams. Flow meters (Rotameter) are used to note the flow of solvent and solute respectively. The continuous and dispersed face streams are metered and derived from separate containers. Each stage consists of a woven wire mesh section and a mixing section. The propeller speed can be controlled to the desired value by a controller. Total set-up is housed in a well-designed rigid structure. The structure also supports tanks, piping, Rotameter, panel and other units.

Learning Objectives/Experiments:
  • To determine overall mass transfer co-efficient based on continuous & dispersed phase.
  • To determine individual `Height of Transfer Unit' based on continuous & dispersed phase.

Required for Operation:
  • Compressed Air Supply at 2 Bar, 0.5 CFM.
  • Water Supply
  • Floor Drain.
  • Electricity Supply: 1 Phase, 220 V AC, 0.5 kW.
  • Required Chemicals & Laboratory Glassware.

Control Panel:
  • Digital RPM Indicator, non contact type with proximity sensor
  • Standard make on/off switch, Mains Indicator etc.

Scope of Delivery:
  • 1 Self-contained “York Scheibel's Column” Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.
  • Photograph is only for reference, final product may vary from it.
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Ion Exchange Apparatus

Ion Exchange Apparatus
 
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Product Details:
Feed CirculationFHP Pump Tullu / Champion make
Column (2 Nos.)Material Borosilicate Glass / Stainless Steel Dia 55mm, Length 500mm approx. (For Anion & Cation)
Bench Area1.2 m x 1 m
Electricity Supply1 Phase, 220 V AC, 0.5 kW
Conductivity MeasurementDigital Conductivity Meter
Size1/4 Inch
Water TankMaterial Stainless Steel, Capacity 25 Ltrs.
Flow MeasurementRotameter, Eureka make
PipingStainless Steel and PVC

Technical Description:
  • The set up consists of two glass column packed with Anion and Cation exchanger resin upto suitable height. The layer of glass wool is placed on bottom and top of the resin bed. The feed is allowed to enter from the bottom of first column and comes out of the top, which is again passed through the second column is same fashion. A digital conductivity meter measures the conductivity of liquid coming out of the second column. Flow rate of water is measured with the pre-calibrated rotameter. A tank with FHP pump with flow control valve and by-pass arrangement is provided for feed circulation. Learning Objectives/Experiments To deionise water to make it soft and to determine the exchange rate and saturation point.

Required for Operation:
  • Required Chemicals & Laboratory Glassware.
  • Required analyzing equipments as per the system to study.

Control Panel:
  • Standard make on/off switch, Mains Indicator etc.

Scope of Delivery:
  • 1 Self-contained 'Ion Exchange' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.
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Experimental Water Cooling Tower Apparatus

Experimental Water Cooling Tower Apparatus
 
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Product Details:
Air CirculationBy forced draft fan, arrangement is done to vary the air flow rate.
PackingExpanded wire mesh.
Temperature sensorsRTD PT-100 type 6 Nos.
Air Flow MeasurementOrifice meter with U-tube manometer.
Dry & Wet Bulb TemperatureMeasured by Temperature Sensors insulated with ceramic fibre wool.

Experimental Water Cooling Tower is a forced draft counter flow type cooling tower specially designed for the Engineering students to provide them insight about actual working of tower. In this system, air from a fan enters at the bottom of the tower and after passing through the mesh packing, discharges into the atmosphere via a duct. Airflow is controlled by a butterfly valve on the blower's delivery line. Water is evenly distributed over the packing by nozzles at top of the tower. Water flow and temperatures can be measured and controlled with suitable instrumentation provided. A water tank at the bottom fitted with level gauge enables to show the exact evaporation loss. Front side acrylic sheet provides actual visualization of cooling tower operation. Air and water flow rates as well as inlet water temperatures can be varied to have different sets of readings.

Learning Objectives/Experiments:
  • Actual visualization of the cooling tower operation.
  • To determine the mass transfer coefficient

Required for Operation:
  • Water Supply & Drain.

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • 0-2000C, for hot water tank.
  • 0-199.90 C, with multi-channel switch

Scope of Delivery:
  • 1 Self-contained 'Experimental Water Cooling Tower' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-25
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Vapour In Air Diffusion Equipment

Vapour In Air Diffusion Equipment
 
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Product Details:
MaterialWith two sides made of glass Capacity 8Ltrs. fitted with heater and stirrer.
StirrerStainless Steel, Impeller and shaft coupled with FHP motor
Digital Temp Controller cum-IndicatorFor Water Bath 0-199.9 deg C
Temperature SensorRTD PT-100 type

Technical Description:
  • Using a small sample of the liquid in a narrow vertical tube, and observing its rate of evaporation into stream of air passed across the top of the tube can conveniently be used to study the diffusion of vapour of a volatile liquid into air. The set up consists of a glass tube placed in a water bath. A horizontal glass tube is fixed to the upper end of the tube and air is drawn through this by a small air pump included within the unit. Air flows over this tube maintaining partial pressure difference. A Traveling microscope with sliding vernier scale is provided to measure the rate of fall of solvent within capillary. A stirrer is fitted to maintain constant temperature inside the bath.

Learning Objectives/Experiments:
  • Determination of the diffusion co-efficient of an organic vapour in air.
  • To study the effect of temperature on diffusion co-efficient.

Required for Operation:
  • Required Chemicals & Laboratory Glassware.
  • Table for setup support
  • The whole set-up is ingeniously designed and schematically arranged on a powder-coated rigid structure

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.

Scope of Delivery:
  • 1 Self-contained 'Vapour In Air Diffusion' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-14
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Simple Batch Distillation Apparatus

Simple Batch Distillation Apparatus
 
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Product Details:
Water SupplyContinuous 4 LPM at 1 Bar
Digital Temp. Indicator0-199.90C with multi-channel switch
Electricity Supply1 Phase, 220 V AC, 2 kW
Design TypeCustomised

The equipment consists of a distillation still made of stainless steel. The feed in the still is heated externally by heater. The vapous form the top of the vessel is condensed in the type condenser by circulating cooling water. Temperature of the feed mixture is controlled by means of a digital temperature Controller. The condensate is collected in a receiver made of stainless steel.

Learning Objectives/Experiments:
  • To study the characteristics of Simple Distillation.
  • To verify of Reyleigh's Equation.

Required for Operation:
  • Floor Drain.
  • Required Chemicals.

Other Details:
  • Flow measurement
  • Rotameter for cold water for condenser
  • Distillation still
  • Made of Stainless Steel, capacity 5ltrs. Insulated with ceramic wool
  • And cladding with Aluminum foil.
  • Condenser
  • Concentric Tube type made of Stainless Steel
  • Distillate tank
  • Made of Stainless Steel, capacity 2 Ltrs.
  • Heater
  • Nichrome wire heater.
  • The whole set-up is ingeniously designed and schematically arranged on a powder-coated rigid structure.

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.
  • Digital Temp. Controller 0-199.9 DegreeC, RTD PT-100 type (For Steam Generator).

Scope of Delivery:
  • 1 Self Contained "Simple Batch Distillation Set-Up" Apparatus.
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-10
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Solid in Air Diffusion Apparatus

Solid in Air Diffusion Apparatus
 
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Product Details:
Compressed Air Supply2 Bar, 4 CFM.
Weighing Balance resolution0.01 gm
Air flow MeasurementRota meter
Diffusion Column MaterialBorosilicate Glass

Confirming a packed bed of spherical balls of a solid in a vertical tube, and observing its rate of diffusion into the stream of air passed across the top of the tube can conveniently study the diffusion of solid into the air. The equipment is fitted with a vertical glass column with a mesh near the base of the column to hold the spherical balls. Spherical balls of known weight and diameter are filled in the column to make a packed bed. Air is allowed to pass through the silica gel chamber. From the bottom of the column, dry air is allowed to enter in the packed bed.

Learning Objectives/Experiments:
  • To calculate the mass transfer coefficient of vaporization of naphthalene in air using a packed bed of spherical particles of naphthalene.
  • To plot Sh/Sc 1/3 Vs Re on log 45g graph and determine the functional relationship.

Required for Operation:
  • Solid Spherical Balls of Naphthalene
  • Table for setup support

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.

Scope of Delivery:
  • 1 Self-contained 'Solid in Air Diffusion Apparatus' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-15
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Absorption in Sieve Plate Column Apparatus

Absorption in Sieve Plate Column Apparatus
 
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Product Details:
Section MaterialOne section of column is provided of Borosilicate glass to visualize the process
Flow MeasurementRotameters (One each for feed, air & CO2)
Collecting TankMaterial Stainless Steel, Capacity 10 Ltrs.
PlatesPerforated Plates made of Stainless Steel (7 Nos.)

Technical Description:
  • The set up consists of a column fitted with perforated plates. Liquid is fed at the top of the column through distributor. The solute gas and air are measured separately, mixed in a mixing chamber and then passed through the perforated plates vertically upward and absorbed in liquid. All the flow rates can be independently varied to simulate different conditions. Liquid Sample can be taken out from the bottom of the column for analysis.

Learning Objectives/Experiments:
  • To study absorption of CO2 in aqueous NaOH solution in a sieve plate column.
  • To determine the gas phase mass transfer co-efficient, KG.

Required for Operation:
  • Water Supply
  • Floor Drain.
  • CO2 cylinder with control valve, pressure regulator and Pressure gauges
  • Required Chemicals & Laboratory Glassware.
  • The whole set-up is ingeniously designed and schematically arranged on a powder-coated rigid structure.

Control Panel:
  • Standard make On/Off switch, Mains Indicator etc.

Scope of Delivery:
  • 1 Self-contained 'Absorption in Sieve Plate Column Apparatus' Apparatus
  • 1 Instruction Manual consisting of experimental procedures, block diagram etc.

Additional Information:
  • Item Code: QMT-11
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YORK SCHREIBER'S EXTRACTION UNIT

YORK SCHREIBER'S EXTRACTION UNIT
 
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The York Schreiber's Column falls in the class of gravity-operated extractors with mechanical agitation. The presence of alternatively agitating and calming sections in a York Schreiber's column yield higher extraction efficiency than the conventional packed column. In the setup a continuous counter current contact between the solvent and solute phases is made which results into extract and affiant streams. Flow meters (Rota meter) are used to note the flow of solvent and solute respectively. The continuous and dispersed face streams are metered and derived from separate containers. Each stage consists of a woven wire mesh section and a mixing section. The propeller speed can be controlled to the desired value by a controller. Total set-up is housed in a well-designed rigid structure. The structure also supports tanks, piping, Rotameter, panel and other units.
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Swenson Walker Crystallizer

Swenson Walker Crystallizer
 
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The set-up is designed to demonstrate and stimulate the phenomena of crystallization. Swenson Walker crystallizer is a continuous type crystallizer. This operation involves both heat and mass transfer. Crystallization is the formation of solid particles within a homogeneous phase. Its wide use has a two-fold basis; a crystal formed from an impure solution is itself pure.
The setup consists of a top open jacketed round bottom trough. A ribbon mixer is provided in crystallizer trough, which rotates at low rpm for agitation of saturated solution. The saturated solution is prepared in a tank fitted with heater and a stirrer. This hot saturated solution is fed at one end of the crystallizer and flows slowly towards the other end while being cooled and is allowed to flow back in hot feed tank making the process continuous. The crystals sediments at the bottom of the trough, and can be washed out at the end of process. Arrangement for Cooling water circulation and flow measurement in jacket is made by using storage type water tank, a pump and a rotameter. Necessary instrumentation is done for temp measurement
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VAPOR IN AIR DIFUSSION APPARATUS

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Using a small sample of the liquid in a narrow vertical tube, and observing its rate of evaporation into stream of air passed across the top of the tube can conveniently be used to study the diffusion of vapour of a volatile liquid into air. The set up consists of a glass tube placed in a water bath. A horizontal glass tube is fixed to the upper end of the tube and air is drawn through this by a small air pump included within the unit. Air flows over this tube maintaining partial pressure difference. A Traveling microscope with sliding vernier scale is provided to measure the rate of fall of solvent within capillary. A stirrer is fitted to maintain constant temperature inside the bath.
 
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SPRAY TOWER

 
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